Difference between revisions of "Calibrations"

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=====Calibration checklist=====
 
=====Calibration checklist=====
  
  * Clean chamber (ultrasonic bath and isopropanol)
+
  * Clean chamber
 
     * Take apart
 
     * Take apart
     * Clean modules
+
     * Clean modules - BOSIMANITE AL-29 followed by ROGYPAL CA-307 Z, bake for 80*C for 18 hours
     * Clean O-rings
+
     * Clean O-rings - Isopropanol
  * Put chamber together (with new modules including LN2 trap, solid bottom plate and central feedthrough)
+
  * Put chamber together (check configuration required)
* Do not touch the surface of the grating or the lamp window with any material! Do not put solvents on it.
 
 
  * Reconnect monochromator
 
  * Reconnect monochromator
 
     * Adjust height to prevent bending of modules during pumping
 
     * Adjust height to prevent bending of modules during pumping
 
     * Connect securely
 
     * Connect securely
  * Clean sample holder (ultrasonic bath and isopropanol)
+
  * Clean sample holder - isopropanol
 
     * Central piece  
 
     * Central piece  
 
     * Three frames
 
     * Three frames
 
     * Three doors
 
     * Three doors
 
     * Suspension support
 
     * Suspension support
* Clean base aluminium sample (ultrasonic bath and isopropanol)
+
    * Screws/springs
* Install temperature sensor
+
  * Clean cooling apparatus - isopropanol
* Install sample holder with aluminium sample (for dark count measurements)
 
  * Clean cooling apparatus (ultrasonic bath and isopropanol)
 
 
     * Cooling braids
 
     * Cooling braids
 
     * Screws/springs
 
     * Screws/springs
 +
* Clean base aluminium sample - isopropanol
 +
* Clean readout equipment which will be inside chamber (wires) - isopropanol
 +
* Clean SiPM holder - isopropanol
 +
* Install temperature sensor
 +
* Install sample holder with samples
 
  * Reconnect cooling apparatus
 
  * Reconnect cooling apparatus
 
     * Cooling braids
 
     * Cooling braids
 
     * Screws/springs
 
     * Screws/springs
* Clean readout equipment which will be inside chamber (wires) (isopropanol)
 
* Clean SiPM holder (ultrasonic bath and isopropanol)
 
 
  * Install SiPM holder
 
  * Install SiPM holder
 
     * Visually test that it is in line
 
     * Visually test that it is in line

Revision as of 14:25, 18 November 2022

Calibration checklist
* Clean chamber
   * Take apart
   * Clean modules - BOSIMANITE AL-29 followed by ROGYPAL CA-307 Z, bake for 80*C for 18 hours
   * Clean O-rings - Isopropanol 
* Put chamber together (check configuration required)
* Reconnect monochromator
   * Adjust height to prevent bending of modules during pumping
   * Connect securely
* Clean sample holder - isopropanol
   * Central piece 
   * Three frames
   * Three doors
   * Suspension support
   * Screws/springs
* Clean cooling apparatus - isopropanol
   * Cooling braids
   * Screws/springs
* Clean base aluminium sample - isopropanol
* Clean readout equipment which will be inside chamber (wires) - isopropanol
* Clean SiPM holder - isopropanol
* Install temperature sensor
* Install sample holder with samples
* Reconnect cooling apparatus
   * Cooling braids
   * Screws/springs
* Install SiPM holder
   * Visually test that it is in line
* Reconnect readout equipment
   * Test to make sure all connections are secure
* Pull vacuum down to e-3mbar
* Take a dark count run with aluminium sample and slits closed
   * 30s measurement time
   * Repeat in and out of the lamp beam if possible
   * With all SiPMs
* Take temperature readouts
* Measure lamp
   * Move grating with motor to calibrate motor control
   * Move grating and measure intensity at each wavelength (in 10nm steps)
   * Compare this to the expected spectrum
   * Repeat for all SiPMs
   * Compare spectra between SiPMs
   * Sweep SiPMs across the beam (in 5mm steps)