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Cleaning and stress tests done to solder flux samples
Cleaning
Each sample was wiped for 30 seconds with the corresponding cleaning agent. In the case Tickopur an ultrasonic bath was used Rovana adds the procedure here.
Analysis Steps for ImageJ
- Open images before & after.
- Image -> Type -> 8-bit
- Select a square frame around sample
- Choose the Threshold values for both pictures that result in matching the percentage on analysed light in the pictures as close as possible. All above threshold = 255, all below = 0.
- Note!!! This threshold includes different percentage of picture light for different pictures.
- Analyze -> Set measurements -> Area, Mean Gray Value, Integrated Density. Area = Total umber of selected pixels. Mean Gray Value = The average intensity of the selected pixels. Integrated Density = Sum of the pixel values in the selection (area x mean gray value)
- Frame the region of interest and right click and choose "Measure".
- Results tab should appear.
- Calculate reduction factor using integrated density: Reduction = ((Before−After)/Before)×100%
Results of Cleaning
- Sample 7: KS115 Isopropanol
Before:
- threshold 20 - included 6.61% of light histogram - area: 148996, mean: 64.895, integrated density: 9669090
After:
- threshold 26 - included 6.51% of light histogram - area: 152096, mean: 57.270, integrated density: 8710545
Reduction = 9.9%
- Sample 9: KS611 Isopropanol
Before:
- threshold 18 - included 7.02% of light histogram - area: 121512, mean: 74.371, integrated density: 9036945
After:
- threshold 16 - included 6.87% of light histogram - area: 120777, mean: 68.187, integrated density: 8235480
Reduction = 8.9%
- Sample 11: 105 96SC Isopropanol
Before:
- threshold 42 - included 7.03% of light histogram - area: 265530, mean: 38.618, integrated density: 10254315
After:
- threshold 45 - included 6.94% of light histogram - area: 280340, mean: 35.841, integrated density: 10047765
Reduction = 2.0%
- Sample 13: KS115 Ethanol
Before:
- threshold 37 - included 6.15% of light histogram - area: 185088, mean: 48.004, integrated density: 8884965
After:
- threshold 19 - included 6.00% of light histogram - area: 195636, mean: 41.743, integrated density: 8166375
Reduction = 8.1%